TY - JOUR
T1 - Synthesis of cyclic sulfamides via one pot alkylation/aza-Michael cascade reaction
AU - Martynova, Sofia D.
AU - Peshkov, Anatoly A.
AU - Yu. Levashova, Ekaterina
AU - Golub, Valeria M.
AU - Avakian, Margarita S.
AU - Sharoyko, Vladimir V.
AU - Kalinin, Stanislav A.
AU - Peshkov, Vsevolod A.
AU - Dar'in, Dmitry V.
N1 - Publisher Copyright:
© 2024 Elsevier Ltd
PY - 2024/9/1
Y1 - 2024/9/1
N2 - A straightforward and transition metal-free method for the synthesis of cyclic sulfamides via base-promoted bis-alkylation of tert-butyl (N-alkylsulfamoyl)carbamates with electron-deficient allyl bromides is described. All obtained cyclic sulfamides underwent successful removal of tert-butoxycarbonyl protecting group.
AB - A straightforward and transition metal-free method for the synthesis of cyclic sulfamides via base-promoted bis-alkylation of tert-butyl (N-alkylsulfamoyl)carbamates with electron-deficient allyl bromides is described. All obtained cyclic sulfamides underwent successful removal of tert-butoxycarbonyl protecting group.
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U2 - 10.1016/j.tetlet.2024.155213
DO - 10.1016/j.tetlet.2024.155213
M3 - Article
AN - SCOPUS:85199947996
SN - 0040-4039
VL - 147
JO - Tetrahedron Letters
JF - Tetrahedron Letters
M1 - 155213
ER -